Technology Process of 4-(2-heptyl-2H-tetrazol-5-yl)phenyl 4-heptyloxybenzoate
There total 5 articles about 4-(2-heptyl-2H-tetrazol-5-yl)phenyl 4-heptyloxybenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
DOI:10.1039/c3tc30966e
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / water; methanol / 12 h / Reflux
1.2: pH 2 / Cooling with ice
2.1: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 24 h / 20 °C
With
dmap; dicyclohexyl-carbodiimide; potassium hydroxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1039/c3tc30966e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 120 °C
2.1: sodium hydroxide / water / 0.5 h / Cooling with ice
3.1: potassium carbonate / acetone / 48 h / Reflux
4.1: potassium hydroxide / water; methanol / 12 h / Reflux
4.2: pH 2 / Cooling with ice
5.1: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 24 h / 20 °C
With
dmap; sodium azide; potassium carbonate; ammonium chloride; dicyclohexyl-carbodiimide; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3tc30966e
