(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

Base Information

Chemical Name:(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal
CAS No.:160537-96-2
Molecular Formula:C₁₅H₂₂O
Molecular Weight:218.339
Hs Code.:

Synonyms:(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

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Technology Process of (2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

There total 5 articles about (2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 160537-95-1
(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenol

: 4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3,6'-epoxy-3-methylbutanal

: 160537-96-2
(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

Guidance literature:: With manganese(IV) oxide; 4 A molecular sieve; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/jm00052a009

Reference yield:

: 51318-62-8
ethyl (E)-4-bromo-3-methyl-2-butenoate

: 160537-96-2
(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Zn, 2.) H₂O / 1.) benzene, reflux, overnight, 2.) benzene, RT, 2 h

2: 98.5 percent / NaOMe / methanol / 1.5 h / Heating

3: 100 percent / LiAlH₄ / diethyl ether / 0.75 h / 0 °C

4: 69 percent / 4 A molecular sieves, MnO₂ / CH₂Cl₂ / 24 h / 0 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; 4 A molecular sieve; water; sodium methylate; zinc; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jm00052a009

Reference yield:

: 7291-87-4
2-isopropyl-3-methyl-2-cyclohexen-1-one

: 160537-96-2
(2Z)-4-(2'-isopropyl-3'-methyl-2'-cyclohexen-1'-ylidene)-3-methyl-2-butenal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Zn, 2.) H₂O / 1.) benzene, reflux, overnight, 2.) benzene, RT, 2 h

2: 98.5 percent / NaOMe / methanol / 1.5 h / Heating

3: 100 percent / LiAlH₄ / diethyl ether / 0.75 h / 0 °C

4: 69 percent / 4 A molecular sieves, MnO₂ / CH₂Cl₂ / 24 h / 0 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; 4 A molecular sieve; water; sodium methylate; zinc; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jm00052a009