2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

Base Information

Chemical Name:2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone
CAS No.:115787-57-0
Molecular Formula:C₁₃H₁₆ClNO₂
Molecular Weight:253.729
Hs Code.:

Synonyms:2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

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Technology Process of 2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

There total 2 articles about 2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 115787-51-4
5-(Chloroacetyl)-2-hydroxybenzaldehyde

: 75-64-9
tert-butylamine

: 115787-57-0
2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

Guidance literature:: In isopropyl alcohol; for 18h; Ambient temperature;
DOI:10.1055/s-1988-27768

Reference yield:

: 90-02-8
salicylaldehyde

: 115787-57-0
2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 16 h / Heating

2: 75 percent / propan-2-ol / 18 h / Ambient temperature

With aluminium trichloride; In dichloromethane; isopropyl alcohol;
DOI:10.1055/s-1988-27768

Reference yield:

: 115787-57-0
2-Chloro-1-<3-<<(1,1-dimethylethyl)imino>methyl>-4-hydroxyphenyl>ethanone

: 18559-94-9,34271-50-6
Salbutamol

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) 12M aq. HCl / 1.) 2-propanol, reflux, 2 h, 2.) 18 h

2: NaOCH₃ / methanol / 0.08 h / 0 °C

3: H₂ / 5percent Pd/c / methanol / 10 h / 3102.9 Torr

With hydrogenchloride; hydrogen; sodium methylate; palladium on activated charcoal; In methanol;
DOI:10.1055/s-1988-27768