benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

Base Information

Chemical Name:benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside
CAS No.:177410-59-2
Molecular Formula:C₂₃H₂₇NO₅
Molecular Weight:397.471
Hs Code.:

Synonyms:benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

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Chemical Property of benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

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Technology Process of benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

There total 4 articles about benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-64-1
acetone

: 195006-98-5
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside

: 177410-59-2
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 504000h;
DOI:10.1016/S0957-4166(00)00498-5

Reference yield:

: 434949-21-0
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-3-phenyl-2-propenoyl)-β-D-allopyranoside

: 177410-59-2
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

2: sodium borohydride / tetrahydrofuran / 20 °C

3: magnesium sulphate / CH₂Cl₂ / 336000 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(01)00562-6

Reference yield:

: 434948-85-3
benzyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

: 177410-59-2
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-isopropylidene-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 48 h / Heating

2: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

3: sodium borohydride / tetrahydrofuran / 20 °C

4: magnesium sulphate / CH₂Cl₂ / 336000 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; tetrabutylammomium bromide; magnesium sulfate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0957-4166(01)00562-6