(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Base Information

Chemical Name:(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate
CAS No.:152298-86-7
Molecular Formula:C₂₅H₃₉NO₄SSi
Molecular Weight:477.74
Hs Code.:

Synonyms:(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Suppliers and Price of (S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Chemical Property:

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Technology Process of (S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

There total 3 articles about (S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 161531-12-0
(S)-1-(3-N,N-dibenzylamino-4-hydroxy)butylmethanesulfonate

: 152298-86-7
(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at -20 ℃; for 2h; Yield given;
DOI:10.1016/S0040-4039(00)79340-3

Reference yield:

: 137428-32-1
(2S)-2-[bis(phenylmethyl)amino]-1,4-butanediol

: 152298-86-7
(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CHCl₃ / 1 h / -20 °C

2: imidazole / dimethylformamide / 2 h / -20 °C

With 1H-imidazole; triethylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)79340-3

Reference yield:

: 159497-65-1
N,N-dibenzylasparaginic acid dibenzyl ester

: 152298-86-7
(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / LiAlH₄ / tetrahydrofuran / 3 h / -78 to -55 deg C

2: Et₃N / CHCl₃ / 1 h / -20 °C

3: imidazole / dimethylformamide / 2 h / -20 °C

With 1H-imidazole; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)79340-3