8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:79832-17-0
Molecular Formula:C₃₄H₃₇NO₅
Molecular Weight:539.671
Hs Code.:

Synonyms:8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

There total 4 articles about 8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8-Benzyloxy-1-(3-benzyloxy-4-methoxy-benzyl)-6,7-dimethoxy-2-methyl-3,4-dihydro-isoquinolinium; iodide

: 79832-17-0
8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1.5h;
DOI:10.1039/P19810002016

Reference yield:

: 5487-33-2
O-benzylhomoisovanillic acid

: 79832-17-0
8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride, DMF / benzene / 1 h / 20 °C

2: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

3: 1.) phorphorus oxychloride / 1.) toluene, reflux, 45 min, 2.) 20 deg C, 18 h

4: sodium borohydride / ethanol / 1.5 h / 0 °C

With sodium tetrahydroborate; oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; trichlorophosphate; In ethanol; dichloromethane; water; benzene;
DOI:10.1039/P19810002016

Reference yield:

: 54313-33-6
2-(3-(benzyloxy)-4-methoxyphenyl)acetyl chloride

: 79832-17-0
8-benzyloxy-1-(3-benzyloxy-4-methoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

2: 1.) phorphorus oxychloride / 1.) toluene, reflux, 45 min, 2.) 20 deg C, 18 h

3: sodium borohydride / ethanol / 1.5 h / 0 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; trichlorophosphate; In ethanol; dichloromethane; water;
DOI:10.1039/P19810002016