1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide

Base Information

• Chemical Name: 1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide
• CAS No.: 94224-93-8
• Molecular Formula: C₄₅H₈₁N₄O₂*I
• Molecular Weight: 837.068

Synonyms:1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide

Chemical Property of 1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide

Chemical Property:

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Technology Process of 1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide

There total 1 articles about 1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1,8,15,22-Tetraazatricyclo<13.13.6.68,22>tetracontan (63702-67-0) + methyl 4-(iodomethyl)benzoate (94224-92-7) → 1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.68,22>tetracontane iodide (94224-93-8)

Guidance literature:

In diethyl ether; at 4 ℃; for 336h;

DOI:10.1021/jo00376a021

Reference yield: 74.0%

1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.68,22>tetracontane iodide (94224-93-8) + methyl iodide (74-88-4) → 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,68,22>tetracontane tetrakis(tetrafluoroborate) (105206-50-6)

Guidance literature:

With sodium carbonate; In acetonitrile; at 70 ℃; for 3h;

DOI:10.1021/jo00376a021

upstream raw materials:

1,8,15,22-Tetraazatricyclo<13.13.6.6^8,22>tetracontan

methyl 4-(iodomethyl)benzoate

Downstream raw materials:

1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)

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