Technology Process of C27H49NO5SiSn
There total 6 articles about C27H49NO5SiSn which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); lithium chloride;
In
toluene;
at 100 ℃;
for 6h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / water; 1,4-dioxane / -2 - 0 °C
2: N,N-dimethylformamide dineopentyl acetal / toluene / 3 h / Reflux
3: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
4: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
5: tetrakis(triphenylphosphine) palladium(0); lithium chloride / toluene / 6 h / 100 °C / Inert atmosphere
With
1H-imidazole; tetrakis(triphenylphosphine) palladium(0); iodine; silver trifluoroacetate; triethylamine; N,N-dimethylformamide dineopentyl acetal; lithium chloride;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
2: tetrakis(triphenylphosphine) palladium(0); lithium chloride / toluene / 6 h / 100 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); iodine; silver trifluoroacetate; lithium chloride;
In
chloroform; toluene;