2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

Base Information

Chemical Name:2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid
CAS No.:182193-38-0
Molecular Formula:C₁₉H₃₀NO₆P
Molecular Weight:399.424
Hs Code.:

Synonyms:2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

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Chemical Property of 2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

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Technology Process of 2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

There total 3 articles about 2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 865703-09-9
2-hydroxyphosphinoylmethyl-4-methyl-pentanoic acid ethyl ester

: 94068-22-1
N,N'-bis(benzyloxycarbonyl)ethane-1,1-diamine

: 182193-38-0
2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

Guidance literature:: With acetic anhydride; toluene-4-sulfonic acid; at 5 - 20 ℃; Reagent/catalyst;
DOI:10.1134/S1070363220040313

Reference yield:

: 87438-94-6
ethyl 2-isobutylacrylate

: 108327-37-3
[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinic acid

: 182193-38-0
2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1) 110 deg C, 1 h, 2) 90 deg C, 4 h;
DOI:10.1021/jo9603439

Reference yield:

: 621-84-1
O-benzyl carbamate

: 182193-38-0
2-(ethyloxycarbonyl)-4-methylamyl-1-(N-benzyloxycarbonyl)aminoethylphosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride; acetic anhydride

2: toluene-4-sulfonic acid; acetic anhydride / 5 - 20 °C

With acetic anhydride; toluene-4-sulfonic acid; acetyl chloride;
DOI:10.1134/S1070363220040313