di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

Base Information

Chemical Name:di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate
CAS No.:345953-47-1
Molecular Formula:C₁₆H₂₃Br₂F₂O₃P
Molecular Weight:492.135
Hs Code.:

Synonyms:di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

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Chemical Property of di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

Chemical Property:

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Technology Process of di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

There total 8 articles about di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 513-35-9
2-methyl-but-2-ene

: 38078-09-0
diethylamino-sulfur trifluoride

: 345953-46-0
di-(tert-butyl)-2-bromo-4-(bromomethyl) benzoylphosphonate

: 345953-47-1
di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

Guidance literature:: With sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In hexane; ethyl acetate;

Reference yield:

: 345953-39-1
2-bromo-4-(bromomethyl)benzoic Acid

: 345953-47-1
di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: BH₃ / tetrahydrofuran

2: MnO₂

3: DMSO; (COCl)2; Et₃N

4: DAST

With manganese(IV) oxide; oxalyl dichloride; borane; dimethyl sulfoxide; triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; 4: Swern oxidation;
DOI:10.1016/j.bmcl.2003.11.048

Reference yield:

: 7697-27-0
2-bromo-4-methylbenzoic acid

: 345953-47-1
di(tert-butyl)[2-bromo-4-(bromomethyl)phenyl] (difluoro)methylphosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: NBS / CCl₄

2: BH₃ / tetrahydrofuran

3: MnO₂

4: DMSO; (COCl)2; Et₃N

5: DAST

With manganese(IV) oxide; N-Bromosuccinimide; oxalyl dichloride; borane; dimethyl sulfoxide; triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; tetrachloromethane; 5: Swern oxidation;
DOI:10.1016/j.bmcl.2003.11.048