di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Base Information

Chemical Name:di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate
CAS No.:345953-48-2
Molecular Formula:C₃₀H₃₄BrF₂O₄P
Molecular Weight:607.472
Hs Code.:

Synonyms:di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Chemical Property:

Purity/Quality:

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Technology Process of di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

There total 9 articles about di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 345953-43-7
4-(bromomethyl)-2-bromobenzaldehyde

: 345953-48-2
di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: DMSO; (COCl)2; Et₃N

2.1: DAST

3.1: potassium tert-butoxide / tetrahydrofuran

3.2: tetrahydrofuran

With oxalyl dichloride; potassium tert-butylate; dimethyl sulfoxide; triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; 2.1: Swern oxidation;
DOI:10.1016/j.bmcl.2003.11.048

Reference yield:

: 345953-39-1
2-bromo-4-(bromomethyl)benzoic Acid

: 345953-48-2
di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: BH₃ / tetrahydrofuran

2.1: MnO₂

3.1: DMSO; (COCl)2; Et₃N

4.1: DAST

5.1: potassium tert-butoxide / tetrahydrofuran

5.2: tetrahydrofuran

With manganese(IV) oxide; oxalyl dichloride; borane; potassium tert-butylate; dimethyl sulfoxide; triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; 4.1: Swern oxidation;
DOI:10.1016/j.bmcl.2003.11.048

Reference yield:

: 345953-41-5
[2-bromo-4-(bromomethyl)phenyl]methanol

: 345953-48-2
di(tert-butyl)[2-bromo-4-(3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: MnO₂

2.1: DMSO; (COCl)2; Et₃N

3.1: DAST

4.1: potassium tert-butoxide / tetrahydrofuran

4.2: tetrahydrofuran

With manganese(IV) oxide; oxalyl dichloride; potassium tert-butylate; dimethyl sulfoxide; triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; 3.1: Swern oxidation;
DOI:10.1016/j.bmcl.2003.11.048