5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

Base Information

Chemical Name:5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine
CAS No.:1449482-14-7
Molecular Formula:C₃₉H₃₈N₂O₇
Molecular Weight:646.74
Hs Code.:

Synonyms:5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

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Chemical Property of 5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

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Technology Process of 5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

There total 4 articles about 5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1320217-78-4
5-(2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1449482-14-7
5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

Guidance literature:: With pyridine; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.3987/COM-12-S(N)68

Reference yield:

: 1449482-10-3
5-[3’,5’-di-O-tert-butyldimethylsilyl-(2’-deoxy-D-ribofuranosyl)]-2-phenoxyacetylaminopyridine

: 1449482-14-7
5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere

2: pyridine / 10 h / 0 - 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.3987/COM-12-S(N)68

Reference yield:

: 950830-66-7
2-amino-5-[3’,5’-di-O-tert-butyldimethylsilyl-(2’-deoxy-D-ribofuranosyl)]pyridine

: 1449482-14-7
5-(5’-O-dimethoxytrityl-2’-deoxy-D-ribofuranosyl)-2-phenoxyacetylaminopyridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 10 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere

3: pyridine / 10 h / 0 - 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.3987/COM-12-S(N)68