N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine)

Base Information

• Chemical Name: N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine)
• CAS No.: 1532526-02-5
• Molecular Formula: C₃₇H₃₇F₃N₄
• Molecular Weight: 594.723

Synonyms:N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine)

Chemical Property of N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine)

Chemical Property:

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Technology Process of N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine)

There total 3 articles about N¹,N^1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N²-mesitylbenzene-1,2-diamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-(2-bromophenyl)-2,4,6-trimethylbenzenamine (937807-95-9) + 5-(trifluoromethyl)benzene-1,3-diamine (368-53-6) → N1,N1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N2-mesitylbenzene-1,2-diamine) (1532526-02-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 100 ℃; for 24h; Schlenk technique; Glovebox;

DOI:10.1021/acs.organomet.9b00337

Reference yield:

1-Bromo-2-iodobenzene (583-55-1) → N1,N1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N2-mesitylbenzene-1,2-diamine) (1532526-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 18 h / 100 °C / Schlenk technique; Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 24 h / 100 °C / Schlenk technique; Inert atmosphere; Glovebox

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene;

DOI:10.1021/acs.organomet.1c00080

Reference yield:

2,4,6-trimethylaniline (88-05-1) → N1,N1'-(5-(trifluoromethyl)-1,3-phenylene)bis(N2-mesitylbenzene-1,2-diamine) (1532526-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 18 h / 100 °C / Schlenk technique; Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 24 h / 100 °C / Schlenk technique; Inert atmosphere; Glovebox

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene;

DOI:10.1021/acs.organomet.1c00080

upstream raw materials:

N-(2-bromophenyl)-2,4,6-trimethylbenzenamine

5-(trifluoromethyl)benzene-1,3-diamine

1-Bromo-2-iodobenzene

2,4,6-trimethylaniline

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