C₆₈H₈₈N₆O₂₄Si

Base Information

Chemical Name:C₆₈H₈₈N₆O₂₄Si
CAS No.:200274-11-9
Molecular Formula:C₆₈H₈₈N₆O₂₄Si
Molecular Weight:1401.56
Hs Code.:

C<sub>68</sub>H<sub>88</sub>N<sub>6</sub>O<sub>24</sub>Si

Synonyms:C₆₈H₈₈N₆O₂₄Si

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Chemical Property of C₆₈H₈₈N₆O₂₄Si

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Technology Process of C₆₈H₈₈N₆O₂₄Si

There total 15 articles about C₆₈H₈₈N₆O₂₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: C₆₂H₇₄N₆O₂₄

: 200274-11-9
C₆₈H₈₈N₆O₂₄Si

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(97)10082-8

Reference yield:

: Acetic acid (4aS,6S,7R,8S,8aR)-8-benzyloxy-2,2-dimethyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

: 200274-11-9
C₆₈H₈₈N₆O₂₄Si

Guidance literature:: Multi-step reaction with 10 steps

1: 99 percent / NIS, TfOH / CH₂Cl₂ / 0.25 h

2: 100 percent / aq. acetic acid / 2 h / 80 °C

3: 96 percent / DMAP, Et₃N / CH₂Cl₂

4: 51 percent / TBDMSOTf / acetonitrile; CH₂Cl₂ / 0.17 h / -50 °C

5: 83 percent / TBAF / tetrahydrofuran / 2 h / 0 °C

6: (COCl)2, DIPEA / dimethylsulfoxide; CH₂Cl₂ / 1 h / -78 °C

7: NaClO₂, NaH₂PO₄, 2-methyl-2-butene / 2-methyl-propan-2-ol / 16 h / Ambient temperature

8: ethanol; methanol

9: 100 percent / aq. acetic acid / 2 h / 80 °C

10: 96 percent / DMAP, Et₃N / CH₂Cl₂

With dmap; sodium chlorite; sodium dihydrogenphosphate; N-iodo-succinimide; 2-methyl-but-2-ene; oxalyl dichloride; trifluorormethanesulfonic acid; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0960-894X(97)10082-8

Reference yield:

: 109914-58-1
methyl 4-O-acetyl-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

: 200274-11-9
C₆₈H₈₈N₆O₂₄Si

Guidance literature:: Multi-step reaction with 10 steps

1: 99 percent / NIS, TfOH / CH₂Cl₂ / 0.25 h

2: 100 percent / aq. acetic acid / 2 h / 80 °C

3: 96 percent / DMAP, Et₃N / CH₂Cl₂

4: 51 percent / TBDMSOTf / acetonitrile; CH₂Cl₂ / 0.17 h / -50 °C

5: 83 percent / TBAF / tetrahydrofuran / 2 h / 0 °C

6: (COCl)2, DIPEA / dimethylsulfoxide; CH₂Cl₂ / 1 h / -78 °C

7: NaClO₂, NaH₂PO₄, 2-methyl-2-butene / 2-methyl-propan-2-ol / 16 h / Ambient temperature

8: ethanol; methanol

9: 100 percent / aq. acetic acid / 2 h / 80 °C

10: 96 percent / DMAP, Et₃N / CH₂Cl₂

With dmap; sodium chlorite; sodium dihydrogenphosphate; N-iodo-succinimide; 2-methyl-but-2-ene; oxalyl dichloride; trifluorormethanesulfonic acid; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0960-894X(97)10082-8