epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

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Chemical Name:epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine
CAS No.:1159108-14-1
Molecular Formula:C₃₅H₄₆N₁₆O₈
Molecular Weight:818.853
Hs Code.:

Synonyms:epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

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Chemical Property of epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

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Technology Process of epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

There total 1 articles about epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1159108-12-9
epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

: 1159108-14-1
epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2009.03.021

Reference yield: 80.0%

: 1159108-14-1
epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

: 202722-92-7
3'-O-Acetyl-5'-oxothymidine

: 1174010-23-1
C₄₇H₅₈N₁₈O₁₄

Guidance literature:: 3'-O-Acetyl-5'-oxothymidine; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tet.2009.04.084

Reference yield: 78.0%

: 1159108-14-1
epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

: 28440-13-3
(3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-oxo-1,6-dihydro-9H-purin-9-yl)tetrahydrofuro[3,4-d][1,3]dioxole-4-carboxylic acid

: 1174010-28-6
C₄₈H₅₈N₂₀O₁₃

Guidance literature:: (3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-oxo-1,6-dihydro-9H-purin-9-yl)tetrahydrofuro[3,4-d][1,3]dioxole-4-carboxylic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tet.2009.04.084