epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

Base Information

• Chemical Name: epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine
• CAS No.: 1159108-12-9
• Molecular Formula: C₄₀H₅₄N₁₆O₁₀
• Molecular Weight: 918.97

Synonyms:epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

Chemical Property of epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

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Technology Process of epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

There total 1 articles about epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine (948916-00-5) + Boc-Lys(Fmoc)-OH (84624-27-1) → epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine (1159108-12-9)

Guidance literature:

Boc-Lys(Fmoc)-OH; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 6h;

DOI:10.1016/j.bmcl.2009.03.021

Reference yield: 84.0%

epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine (1159108-12-9) → epi-5-N[[[αN-(tert-butoxycarbonyl)]lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine (1174010-22-0)

Guidance literature:

With diethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

DOI:10.1016/j.tet.2009.04.084

Reference yield: 76.0%

epi-5-N[[[αN-(tert-butoxycarbonyl)-εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine (1159108-12-9) → epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine (1159108-14-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1016/j.bmcl.2009.03.021

upstream raw materials:

epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine

Boc-Lys(Fmoc)-OH

Downstream raw materials:

epi-5-N[[[εN-(9-fluorenylmethyloxycarbonyl)]-lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

epi-5-N[[[αN-(tert-butoxycarbonyl)]lysinyl]aminoethyl]-1,3,2',6'-tetraazido neamine

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