3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

Base Information

Chemical Name:3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide
CAS No.:454464-57-4
Molecular Formula:C₁₇H₁₅ClN₄OS
Molecular Weight:358.851
Hs Code.:

3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3<i>H</i>-imidazol-4-yl]-benzamide

Synonyms:3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

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Chemical Property of 3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

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Technology Process of 3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

There total 6 articles about 3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 454464-58-5
3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzoic acid methyl ester

: 454464-57-4
3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

Guidance literature:: With ammonia; In methanol; for 48h;
DOI:10.1021/jm0211117

Reference yield:

: 19829-31-3
1-(3-bromophenyl)-1-propanone

: 454464-57-4
3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: 81 percent / dimethylformamide / 6 h / Heating

2.1: KOH / ethanol / 2 h / Heating

3.1: H₂SO₄

4.1: 100 percent / Br₂ / 0.33 h / 20 °C

5.1: AcOH / 0.5 h

5.2: 90 percent / AcOH

6.1: 73 percent / NH₃ / methanol / 48 h

With potassium hydroxide; sulfuric acid; ammonia; bromine; acetic acid; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0211117

Reference yield:

: 74380-71-5
3-hydroxycarbonyl-propiophenone

: 454464-57-4
3-[3-(3-chloro-phenylamino)-2-mercapto-5-methyl-3H-imidazol-4-yl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: H₂SO₄

2.1: 100 percent / Br₂ / 0.33 h / 20 °C

3.1: AcOH / 0.5 h

3.2: 90 percent / AcOH

4.1: 73 percent / NH₃ / methanol / 48 h

With sulfuric acid; ammonia; bromine; acetic acid; In methanol;
DOI:10.1021/jm0211117