1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

Base Information

Chemical Name:1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene
CAS No.:1392322-55-2
Molecular Formula:C₂₅H₃₆O₆
Molecular Weight:432.557
Hs Code.:

Synonyms:1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

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Chemical Property of 1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

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Technology Process of 1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

There total 10 articles about 1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1392322-54-1
(E)-1-(4-Isopropoxy-2,3,6-trimethoxyphenyl)-3-(4-isopropoxy-3-methoxyphenyl)prop-2-en-1-one

: 1392322-55-2
1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

Guidance literature:: With triethylsilane; trifluoroacetic acid; at 20 ℃; for 4h;
DOI:10.1248/cpb.60.557

Reference yield:

: 1392322-52-9
1-isopropoxy-2,3,5-trimethoxybenzene

: 1392322-55-2
1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: tin(IV) chloride / dichloromethane / 20 °C

2: sodium hydroxide / methanol / 12 h / 20 °C

3: triethylsilane; trifluoroacetic acid / 4 h / 20 °C

With triethylsilane; tin(IV) chloride; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; 1: Friedel Crafts acylation / 2: Aldol condensation;
DOI:10.1248/cpb.60.557

Reference yield:

: 2973-76-4
5-bromo-4-hydroxy-3-methoxybenzaldehyde

: 1392322-55-2
1-isopropoxy-4-(3-(4-isopropoxy-3-methoxyphenyl)propyl)-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 8 steps

1.1: copper; sodium hydroxide / water / 24 h / Reflux

2.1: acetone / 6 h / Reflux; Alkaline conditions

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

4.2: 2 h / 20 °C

5.1: potassium hydroxide / methanol / 48 h / 20 °C

6.1: tin(IV) chloride / dichloromethane / 20 °C

7.1: sodium hydroxide / methanol / 12 h / 20 °C

8.1: triethylsilane; trifluoroacetic acid / 4 h / 20 °C

With triethylsilane; tin(IV) chloride; copper; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 4.1: Baeyer-Villiger oxidation / 6.1: Friedel Crafts acylation / 7.1: Aldol condensation;
DOI:10.1248/cpb.60.557