1-isopropoxy-2,3,5-trimethoxybenzene

Base Information

Chemical Name:1-isopropoxy-2,3,5-trimethoxybenzene
CAS No.:1392322-52-9
Molecular Formula:C₁₂H₁₈O₄
Molecular Weight:226.273
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-isopropoxy-2,3,5-trimethoxybenzene

Chemical Property:

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Technology Process of 1-isopropoxy-2,3,5-trimethoxybenzene

There total 5 articles about 1-isopropoxy-2,3,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₆O₄

: 74-88-4
methyl iodide

: 1392322-52-9
1-isopropoxy-2,3,5-trimethoxybenzene

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 48h;
DOI:10.1248/cpb.60.557

Reference yield:

: 195506-21-9
3-isopropoxy-4,5-dimethoxybenzaldehyde

: 1392322-52-9
1-isopropoxy-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

1.2: 2 h / 20 °C

2.1: potassium hydroxide / methanol / 48 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In methanol; dichloromethane; 1.1: Baeyer-Villiger oxidation;
DOI:10.1248/cpb.60.557

Reference yield:

: 2973-76-4
5-bromo-4-hydroxy-3-methoxybenzaldehyde

: 1392322-52-9
1-isopropoxy-2,3,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper; sodium hydroxide / water / 24 h / Reflux

2.1: acetone / 6 h / Reflux; Alkaline conditions

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

4.2: 2 h / 20 °C

5.1: potassium hydroxide / methanol / 48 h / 20 °C

With copper; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 4.1: Baeyer-Villiger oxidation;
DOI:10.1248/cpb.60.557