tert-Butyl pyridin-3-ylcarbamate

Base Information Edit

Chemical Name:tert-Butyl pyridin-3-ylcarbamate
CAS No.:56700-70-0
Molecular Formula:C10H14 N2 O2
Molecular Weight:194.233
Hs Code.:2933399090
European Community (EC) Number:627-758-0
DSSTox Substance ID:DTXSID60448782
Nikkaji Number:J1.848.094H
Wikidata:Q72448405
Mol file:56700-70-0.mol

Synonyms:tert-Butyl pyridin-3-ylcarbamate;56700-70-0;3-(Boc-amino)pyridine;3-tert-Butoxycarbonylaminopyridine;Tert-butyl N-pyridin-3-ylcarbamate;3-(tert-butoxycarbonylamino)pyridine;TERT-BUTYL N-(PYRIDIN-3-YL)CARBAMATE;tert-Butyl (pyridin-3-yl)carbamate;MFCD02179231;CARBAMIC ACID, 3-PYRIDINYL-, 1,1-DIMETHYLETHYL ESTER;3-(Boc-amino)-pyridine;tert-butyl N-(3-pyridyl)carbamate;3-Boc-aMinopyridine;SCHEMBL349933;t-butyl pyridine-3-ylcarbamate;tert-butyl 3-pyridinylcarbamate;tert-Butylpyridin-3-ylcarbamate;3-(Boc-amino)pyridine, 97%;3-(t-butoxycarbonylamino)pyridine;DTXSID60448782;WKHGDPZRLXDVMJ-UHFFFAOYSA-N;AMY32298;CS-M1308;3-(t-butyloxycarbonyl)amino pyridine;AB6784;3-(tert-butoxycarbonyl amino)pyridine;AKOS013153306;AB11052;AC-5745;3-Pyridinylcarbamic acid tert-butyl ester;AC-27334;SY006287;FT-0646341;(pyridin-3-yl)-carbamic acid tert-butyl ester;A831148;J-510820;PYRIDIN-3-YL-CARBAMIC ACID TERT-BUTYL ESTER

Suppliers and Price of tert-Butyl pyridin-3-ylcarbamate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-ButylPyridin-3-ylcarbamate
100mg
$ 75.00

SynChem
Pyridin-3-yl-carbamic acid tert-butyl ester 95+%
10 g
$ 165.00

SynChem
Pyridin-3-yl-carbamic acid tert-butyl ester 95+%
1 g
$ 30.00

SynChem
Pyridin-3-yl-carbamic acid tert-butyl ester 95+%
5 g
$ 95.00

Sigma-Aldrich
3-(Boc-amino)pyridine 97%
1g
$ 47.60

Sigma-Aldrich
3-(Boc-amino)pyridine 97%
10g
$ 237.00

Oakwood
tert-Butylpyridin-3-ylcarbamate 95%
25g
$ 259.00

Labseeker
3-(tert-Butoxycarbonylamino)pyridine 95
25g
$ 385.00

Crysdot
tert-Butylpyridin-3-ylcarbamate 98%
100g
$ 644.00

Crysdot
tert-Butylpyridin-3-ylcarbamate 98%
25g
$ 257.00

Total 49 raw suppliers

Chemical Property of tert-Butyl pyridin-3-ylcarbamate Edit

Chemical Property:

Vapor Pressure:0.019mmHg at 25°C
Melting Point:116-120ºC
Refractive Index:1.544
Boiling Point:252.743 °C at 760 mmHg
PKA:12.93±0.70(Predicted)
Flash Point:106.656 °C
PSA：51.22000
Density:1.131
LogP:2.50160
Storage Temp.:Keep in dark place,Sealed in dry,Room Temperature
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:194.105527694
Heavy Atom Count:14
Complexity:199

Purity/Quality:

98%,99%, ^*data from raw suppliers

tert-ButylPyridin-3-ylcarbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-43
Safety Statements: 36/37

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC1=CN=CC=C1

Technology Process of tert-Butyl pyridin-3-ylcarbamate

There total 10 articles about tert-Butyl pyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 462-08-8
pyridin-3-ylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 56700-70-0
3-(tert-butoxycarbonylamino)pyridine

Guidance literature:: pyridin-3-ylamine; With sodium hexamethyldisilazane; In tetrahydrofuran; for 1.5h; Inert atmosphere;

di-tert-butyl dicarbonate; In tetrahydrofuran; for 19h; Inert atmosphere;

Reference yield: 92.0%

: 22236-96-0
3-N-formylaminopyridine

: 75-65-0
tert-butyl alcohol

: 56700-70-0
3-(tert-butoxycarbonylamino)pyridine

Guidance literature:: With lead(IV) acetate; In tetrachloromethane; for 0.25h; Heating;
DOI:10.1055/s-1982-29757

Reference yield: 91.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 4248-19-5
tert-butyl carbazate

: 56700-70-0
3-(tert-butoxycarbonylamino)pyridine

Guidance literature:: With ?di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate; In water; at 50 ℃; for 24h; Inert atmosphere; Green chemistry;
DOI:10.1039/c3gc42188k