tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

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Chemical Name:tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside
CAS No.:1092935-44-8
Molecular Formula:C₂₇H₃₇N₃O₆Si
Molecular Weight:527.693
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

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Chemical Property of tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

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Technology Process of tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

There total 1 articles about tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: tert-butyldimethylsilyl-2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

: 100-39-0
benzyl bromide

: 1092935-44-8
tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

Guidance literature:: tert-butyldimethylsilyl-2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h;

benzyl bromide; In tetrahydrofuran; mineral oil; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2008.06.011

Reference yield: 88.0%

: 1092935-44-8
tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

: 1092935-46-0
tert-butyldimethylsilyl 2-azido-3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: With sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 9.66h; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2008.06.011