(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Base Information

Chemical Name:(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol
CAS No.:1342341-39-2
Molecular Formula:C₁₆H₁₈BrNO₃S
Molecular Weight:384.294
Hs Code.:

Synonyms:(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Suppliers and Price of (Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

There total 4 articles about (Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1342341-38-1
methyl (Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-enoate

: 1342341-39-2
(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; for 3h; Cooling;
DOI:10.1055/s-0030-1260098

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 1342341-39-2
(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloroform / 12 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / Cooling

2.2: 0.5 h / Cooling

3.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / Cooling

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; chloroform; mineral oil;
DOI:10.1055/s-0030-1260098

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 1342341-39-2
(Z)-2-bromo-3-[1-(2,4,6-trimethylphenylsulfonyl)-1H-pyrrol-2-yl]prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / Cooling

1.2: 0.5 h / Cooling

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / Cooling

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1055/s-0030-1260098