Technology Process of C17H18FNO4
There total 3 articles about C17H18FNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
9-(2-mesityl)-10-methylacridinium perchlorate;
In
1,2-dichloro-ethane;
at 20 ℃;
for 40h;
Irradiation;
Schlenk technique;
DOI:10.1002/anie.201400602
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydroxylamine hydrochloride; sodium acetate / methanol; water / 20 °C
2.1: triethylamine; methanesulfonyl chloride / tetrahydrofuran / 0.5 h / 0 - 20 °C
2.2: 0.52 h
3.1: 9-(2-mesityl)-10-methylacridinium perchlorate / 1,2-dichloro-ethane / 40 h / 20 °C / Irradiation; Schlenk technique
With
hydroxylamine hydrochloride; sodium acetate; methanesulfonyl chloride; triethylamine; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
tetrahydrofuran; methanol; water; 1,2-dichloro-ethane;
DOI:10.1002/anie.201400602
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; methanesulfonyl chloride / tetrahydrofuran / 0.5 h / 0 - 20 °C
1.2: 0.52 h
2.1: 9-(2-mesityl)-10-methylacridinium perchlorate / 1,2-dichloro-ethane / 40 h / 20 °C / Irradiation; Schlenk technique
With
methanesulfonyl chloride; triethylamine; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1002/anie.201400602