Technology Process of BIS(DODECYLCYCLOPENTADIENYL)ZIRCONIUM(IV) DICHLORIDE
There total 1 articles about BIS(DODECYLCYCLOPENTADIENYL)ZIRCONIUM(IV) DICHLORIDE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
CpMgCl; 1-dodecylbromide;
In
tetrahydrofuran;
at 60 ℃;
for 6h;
Inert atmosphere;
With
n-butyllithium;
In
hexanes; diethyl ether;
at 20 ℃;
for 0.666667h;
Inert atmosphere;
zirconium(IV) chloride;
In
hexanes; diethyl ether;
at 20 ℃;
for 3h;
Inert atmosphere;