1-chlorocyclopropyl p-methoxyphenyl sulfide

Base Information

Chemical Name:1-chlorocyclopropyl p-methoxyphenyl sulfide
CAS No.:76042-11-0
Molecular Formula:C₁₀H₁₁ClOS
Molecular Weight:214.716
Hs Code.:

Synonyms:1-chlorocyclopropyl p-methoxyphenyl sulfide

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Chemical Property of 1-chlorocyclopropyl p-methoxyphenyl sulfide

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Technology Process of 1-chlorocyclopropyl p-methoxyphenyl sulfide

There total 1 articles about 1-chlorocyclopropyl p-methoxyphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 69563-32-2
1-(cyclopropylsulphanyl)-4-methoxybenzene

: 76042-11-0
1-chlorocyclopropyl p-methoxyphenyl sulfide

Guidance literature:: With N-chloro-succinimide; In benzene; for 23h; Ambient temperature;
DOI:10.1021/ja00547a015

Reference yield: 56.0%

: 76042-11-0
1-chlorocyclopropyl p-methoxyphenyl sulfide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 76042-12-1
1-((p-methoxyphenyl)thio)cyclopropane-1-carboxaldehyde

Guidance literature:: With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 0.5h;
DOI:10.1021/ja00547a015

Reference yield:

: 76042-11-0
1-chlorocyclopropyl p-methoxyphenyl sulfide

: 76042-36-9
1-Butyl-2-[1-[1-(4-methoxy-phenylsulfanyl)-cyclopropyl]-meth-(E)-ylidene]-cyclohexanol

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / tert-butyllithium / diethyl ether; pentane / 0.5 h / -78 °C

2: 83 percent / lithium diisopropylamide / tetrahydrofuran / -78 °C

3: 1.) phosphorus oxychloride, HMPA, 2.) pyridine / 1.) room temperature -> 50 deg C, 2.) 50 deg C -> 100 deg C

4: 70 percent / diethyl ether / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; lithium diisopropyl amide; trichlorophosphate; In tetrahydrofuran; diethyl ether; pentane;
DOI:10.1021/ja00547a015