N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

Base Information

Chemical Name:N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide
CAS No.:1337864-58-0
Molecular Formula:C₁₆H₂₀N₄O₃
Molecular Weight:316.36
Hs Code.:

Synonyms:N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

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Chemical Property of N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

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Technology Process of N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

There total 3 articles about N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1065104-32-6
2-(3-methyl-6-oxo-5,6-dihydropyridazin-1-(4H)-yl)acetohydrazide

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1337864-58-0
N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

Guidance literature:: With hydrogenchloride; In ethanol; water; at 20 ℃; for 2h;
DOI:10.1007/s00044-011-9770-6

Reference yield:

: 3128-06-1
5-ketohexanoic acid

: 1337864-58-0
N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / Reflux

2.1: potassium carbonate / acetone / 4 h / Reflux

2.2: 2 h / Reflux

3.1: hydrazine hydrate / ethanol / 1 h / Reflux

4.1: hydrogenchloride / ethanol; water / 2 h / 20 °C

With hydrogenchloride; potassium carbonate; hydrazine hydrate; In ethanol; water; acetone;
DOI:10.1007/s00044-011-9770-6

Reference yield:

: 5157-08-4
3-methyl-4,5-dihydro-6-oxopyridazine

: 1337864-58-0
N'-(1-(4-methoxyphenyl)ethylidene)-2-(3-methyl-6-oxo-5,6-dihydropyridazin-1(4H)-yl)acetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 4 h / Reflux

1.2: 2 h / Reflux

2.1: hydrazine hydrate / ethanol / 1 h / Reflux

3.1: hydrogenchloride / ethanol; water / 2 h / 20 °C

With hydrogenchloride; potassium carbonate; hydrazine hydrate; In ethanol; water; acetone;
DOI:10.1007/s00044-011-9770-6