7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene

Base Information

• Chemical Name: 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene
• CAS No.: 57770-87-3
• Molecular Formula: C₂₂H₂₄N₂O₂
• Molecular Weight: 348.445

Synonyms:7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene

Chemical Property of 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene

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Technology Process of 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene

There total 6 articles about 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.5%

2,6-bis(4-methoxybenzylidene)cyclohexanone (62085-71-6,6275-32-7) → 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene (57770-87-3)

Guidance literature:

With hydrazine hydrate; In methanol; for 1.5h; Heating;

Reference yield: 72.0%

(2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone (6275-32-7,62085-71-6) → 7-p-methoxyphenyl-2-p-methoxyphenylmethylene-8,9-diazabicyclo[4.3.0]non-9-ene (57770-87-3)

Guidance literature:

With hydrazine hydrate; In ethanol;

DOI:10.1055/s-2002-33917

Reference yield:

(2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone (6275-32-7,62085-71-6) → (7E)-3-(4-methoxyphenyl)-7-[(4-methoxyphenyl)methylidene]-3,3a,4,5,6,7-hexahydro-2H-indazole (57770-87-3)

Guidance literature:

With hydrazine hydrate; In ethanol; Heating;

DOI:10.1134/S1070428016030167

upstream raw materials:

(2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone

2,6-bis(4-methoxybenzylidene)cyclohexanone

cyclohexanone

4-methoxy-benzaldehyde

Downstream raw materials:

2-acetyl-7-(4-methoxy-benzylidene)-3-(4-methoxy-phenyl)-3,3a,4,5,6,7-hexahydro-2H-indazole

(3R,3aS)-3-(4-Methoxy-phenyl)-7-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-3,3a,4,5,6,7-hexahydro-indazole-2-carbodithioic acid

(3R,3aS)-3-(4-Methoxy-phenyl)-7-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-2-nitroso-3,3a,4,5,6,7-hexahydro-2H-indazole

{(3R,3aS)-3-(4-Methoxy-phenyl)-7-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-3,3a,4,5,6,7-hexahydro-indazol-2-yl}-methanol

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