N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester
CAS No.:158629-47-1
Molecular Formula:C₄₀H₅₀N₄O₉
Molecular Weight:730.858
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

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Chemical Property of N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

Chemical Property:

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Technology Process of N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

There total 6 articles about N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5616-81-9
sarcosine tert-butyl ester

: 158629-47-1
N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

2: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

3: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

4: 85percent aq. formic acid / 4 h / 20 °C

5: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

With formic acid; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00097a003

Reference yield:

: 5616-82-0
N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

: 158629-47-1
N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

2: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

3: 85percent aq. formic acid / 4 h / 20 °C

4: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

With formic acid; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00097a003

Reference yield:

: 101644-79-5
α-tert-butyl N-(benzyloxycarbonyl)-N-methylglycinate

: 158629-47-1
N-(benzyloxycarbonyl)threonyl-D-(O-benzyl)tyrosylprolylsarcosine tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

2: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

3: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

4: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

5: 85percent aq. formic acid / 4 h / 20 °C

6: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

With formic acid; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00097a003