(1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

Base Information

Chemical Name:(1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol
CAS No.:121239-64-3
Molecular Formula:C₁₉H₂₃N₅O₄
Molecular Weight:385.423
Hs Code.:

Synonyms:(1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

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Chemical Property of (1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

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Technology Process of (1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

There total 12 articles about (1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121239-67-6
Acetic acid (1S,2S,3R,4S,6S)-3-acetoxy-4-acetoxymethyl-6-(6-benzoylamino-purin-9-yl)-2-benzyloxy-cyclohexyl ester

: 121239-64-3
(1R,2S,3S,4S,6S)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: With sodium methylate; In methanol; at 23 ℃; for 8h;
DOI:10.1248/cpb.37.542

Reference yield:

: 121239-61-0
Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

: 121239-64-3
(1R,2S,3S,4R,6R)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: With sodium methylate; In methanol; at 23 ℃; for 8h;
DOI:10.1248/cpb.37.542

Reference yield:

: 121239-65-4
Acetic acid (1R,2S,5S,6R)-5-acetoxy-2-acetoxymethyl-6-benzyloxy-3-nitro-cyclohex-3-enyl ester

: 121239-64-3
(1R,2S,3S,4S,6S)-4-(6-Amino-purin-9-yl)-2-benzyloxy-6-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / KF / 18-crown-6 / dimethylformamide / 1 h / 2 °C

2: 77 percent / (n-Bu)3SnH, α,α'-azobis-iso-butyronitrile / benzene / 3 h / 80 °C

3: 1 percent NaOMe / methanol / 8 h / 23 °C

With potassium fluoride; azobisisobutyronitrile; tri-n-butyl-tin hydride; sodium methylate; 18-crown-6 ether; In methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.542