Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

Base Information

Chemical Name:Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester
CAS No.:121239-61-0
Molecular Formula:C₃₇H₃₅N₅O₈
Molecular Weight:677.714
Hs Code.:

Synonyms:Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

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Chemical Property of Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

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Technology Process of Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

There total 3 articles about Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 121239-59-6
Benzoic acid (1R,2R,3S,4S,5R,6S)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-6-nitro-cyclohexylmethyl ester

: 121239-61-0
Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 3h;
DOI:10.1248/cpb.37.542

Reference yield:

: 119951-72-3,120021-17-2
Benzoic acid (1R,4S,5R,6R)-4,6-diacetoxy-5-benzyloxy-2-nitro-cyclohex-2-enylmethyl ester

: 121239-61-0
Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KF / 18-crown-6 / dimethylformamide / 1 h / 2 °C

2: 76 percent / (n-Bu)3SnH, α,α'-azobis-iso-butyronitrile / benzene / 3 h / 80 °C

With potassium fluoride; azobisisobutyronitrile; tri-n-butyl-tin hydride; 18-crown-6 ether; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.542

Reference yield:

: 4005-49-6
N-benzoyladenine

: 121239-61-0
Benzoic acid (1R,2R,3S,4S,5R)-2,4-diacetoxy-5-(6-benzoylamino-purin-9-yl)-3-benzyloxy-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KF / 18-crown-6 / dimethylformamide / 1 h / 2 °C

2: 76 percent / (n-Bu)3SnH, α,α'-azobis-iso-butyronitrile / benzene / 3 h / 80 °C

With potassium fluoride; azobisisobutyronitrile; tri-n-butyl-tin hydride; 18-crown-6 ether; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.542