(1S)-(-)-Camphanic acid amide

Base Information

• Chemical Name: (1S)-(-)-Camphanic acid amide
• CAS No.: 54200-37-2
• Molecular Formula: C₁₀H₁₅NO₃
• Molecular Weight: 197.234
• Hs Code.: 2932209090
• Mol file: 54200-37-2.mol

Synonyms:Camphanicacid amide;(1S,4R)-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carboxamide;2-oxabicyclo[2.2.1]heptane-1-carboxamide, 4,7,7-trimethyl-3-oxo-, (1S,4R)-;

Chemical Property of (1S)-(-)-Camphanic acid amide

Chemical Property:

• Vapor Pressure: 2.16E-06mmHg at 25°C
• Refractive Index: 1.533
• Boiling Point: 393.3 °C at 760 mmHg
• Flash Point: 217.7 °C
• PSA: 69.39000
• Density: 1.239 g/cm³
• LogP: 1.29390

Purity/Quality:

99.0% ^*data from raw suppliers

(1R,4S)-1,7,7-trimethyl-2-oxo-3-oxabicyclo[2.2.1]heptane-4-carboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1S)-(-)-Camphanic acid amide

There total 7 articles about (1S)-(-)-Camphanic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Bromcamphersaeureanhydrid (112924-25-1) → 4,7,7-trimethyl-3-oxo-2-oxa-bicyclo[2.2.1]heptane-1-carboxylic acid amide (54200-37-2)

Guidance literature:

With chloroform; ammonia; amide of/the/ levorotatory w-camphanoic acid;

Reference yield:

3-chloro-3-cyano-1,2,2-trimethyl-cyclopentanecarboxylic acid (871882-83-6) → 4,7,7-trimethyl-3-oxo-2-oxa-bicyclo[2.2.1]heptane-1-carboxylic acid amide (54200-37-2)

Guidance literature:

With alkali; amide;

Reference yield:

→ 4,7,7-trimethyl-3-oxo-2-oxa-bicyclo[2.2.1]heptane-1-carboxylic acid amide (54200-37-2)

Guidance literature:

With ammonium hydroxide; amide of/the/ levorotatory w-camphanoic acid;

upstream raw materials:

3-chloro-3-cyano-1,2,2-trimethyl-cyclopentanecarboxylic acid

4,7,7,-trimethyl-3-oxo-2-oxa-norbornane-1-carboxylic acid nitrile, (nitrile of ω-camphanoic acid )

α-Brom-camphersaeure-anhydrid

Bromcamphersaeureanhydrid