1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE

Base Information

Chemical Name:1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE
CAS No.:13441-28-6
Molecular Formula:C₁₀H₁₃BrO₃
Molecular Weight:261.115
Hs Code.:2917209090
Mol file:13441-28-6.mol

Synonyms:1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE

Suppliers and Price of 1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE 95.00%
10MG
$ 703.40

Total 3 raw suppliers

Chemical Property of 1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE

Chemical Property:

PSA：43.37000
LogP:2.02980

Purity/Quality:

99% ^*data from raw suppliers

1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE

There total 7 articles about 1-BROMO-5,8,8-TRIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-Bromo-2,2,3-trimethyl-cyclopentane-1,3-dicarbonyl dichloride

: 10333-96-7,13441-28-6,112924-25-1
1-Bromo-5,8,8-trimethyl-3-oxa-bicyclo[3.2.1]octane-2,4-dione

Guidance literature:: With water; for 2h; Yield given; temp. below 30 deg C;

Reference yield:

: 13441-28-6
α-Brom-camphersaeure-anhydrid

Guidance literature:: With phosphorus pentachloride; trichlorophosphate; Behandeln mit Brom, anschliessend mit Wasser; Erwaermen des Reaktionsprodukts mit waessr. Essigsaeure;

Reference yield:

: 48138-74-5
1,2,2-trimethyl-cyclopentane-1,3-dicarbonyl chloride

: 10333-96-7,13441-28-6,112924-25-1
1-Bromo-5,8,8-trimethyl-3-oxa-bicyclo[3.2.1]octane-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / 23 h / 65 °C

2: water / 2 h / temp. below 30 deg C

With water; bromine;