N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester

Base Information

Chemical Name:N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester
CAS No.:4864-40-8
Molecular Formula:C₂₇H₃₅N₃O₇
Molecular Weight:513.591
Hs Code.:

<i>N</i><sup>δ</sup>-benzyloxycarbonyl-<i>N</i><sup>α</sup>-(<i>N</i>-benzyloxycarbonyl-valyl)-ornithine methyl ester

Synonyms:N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester

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Chemical Property of N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester

Chemical Property:

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Technology Process of N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester

There total 6 articles about N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2443-71-2
benzyl (S)-(1-hydrazineyl-3-methyl-1-oxobutan-2-yl)carbamate

: 4864-40-8
N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-valyl)-ornithine methyl ester

Guidance literature:: With hydrogenchloride; acetic acid; sodium nitrite; at 0 ℃; N^δ-benzyloxycarbonyl-N^α-<N-benzyloxycarbonyl-L-valyl>-(Ξ)-ornithine methyl ester; Umsetzung des gebildeten Azids mit N^δ-Benzyloxycarbonyl-DL-ornithin-methylester in Aethylacetat;
DOI:10.1038/161804b0

Reference yield:

: 87052-60-6
Z-(S)-Val-Cl

: 4864-40-8
N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-L-valyl)-L-ornithine methyl ester

Guidance literature:: With diethyl ether; potassium hydrogencarbonate; ethyl acetate;

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 4864-40-8
N^δ-benzyloxycarbonyl-N^α-(N-benzyloxycarbonyl-L-valyl)-L-ornithine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous NaOH

2: diethyl ether; PCl₅

3: aqueous KHCO₃; diethyl ether; ethyl acetate

With sodium hydroxide; diethyl ether; phosphorus pentachloride; potassium hydrogencarbonate; ethyl acetate;