N-CBZ-l-valine hydrazine

Base Information

Chemical Name:N-CBZ-l-valine hydrazine
CAS No.:2443-71-2
Molecular Formula:C13H19N3O3
Molecular Weight:265.312
Hs Code.:
DSSTox Substance ID:DTXSID401246978
Nikkaji Number:J1.738.419H
Mol file:2443-71-2.mol

Synonyms:N-CBZ-l-valine hydrazine;SCHEMBL9608964;LIBHJAFLPOAKHL-NSHDSACASA-N;DTXSID401246978;N-(Benzyloxycarbonyl)valine hydrazide;N-[(Phenylmethoxy)carbonyl]-L-valine hydrazide;Benzyl 1-(hydrazinocarbonyl)-2-methylpropylcarbamate #;2443-71-2

Suppliers and Price of N-CBZ-l-valine hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-CBZ-l-valine hydrazine

Chemical Property:

XLogP3:0.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:265.14264148
Heavy Atom Count:19
Complexity:302

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)C(C(=O)NN)NC(=O)OCC1=CC=CC=C1
Isomeric SMILES:CC(C)[C@@H](C(=O)NN)NC(=O)OCC1=CC=CC=C1

Technology Process of N-CBZ-l-valine hydrazine

There total 20 articles about N-CBZ-l-valine hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24210-19-3
methyl (2S)-3-methyl-[(benzyloxy)carbonylamino]butanoate

: 2443-71-2
benzyl (S)-(1-hydrazineyl-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/d0cc02728f

Reference yield: 94.0%

: 68199-62-2,95422-60-9,5564-00-1
<(benzyloxycarbonyl)-L-valinyl>hydrazinecarboxylic acid tert-butyl ester

: 2443-71-2
benzyl (S)-(1-hydrazineyl-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(02)00490-8

Reference yield: 50.5%

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 2443-71-2
benzyl (S)-(1-hydrazineyl-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: (S)-N-(benzyloxycarbonyl)valine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.5h;

With hydrazine hydrate; In dichloromethane; at 0 - 20 ℃; for 2h;