N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

Base Information

Chemical Name:N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide
CAS No.:83892-13-1
Molecular Formula:C₄₁H₅₄N₆O₈
Molecular Weight:758.915
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

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Chemical Property of N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

There total 9 articles about N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40847-02-7
H₂N-L-Leu-NH(n-Bu)

: 83892-13-1
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

Guidance literature:: Multi-step reaction with 3 steps

1: HOBt, DCCI / ethyl acetate / 12 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 7 h

3: HOBt, DCCI / dimethylformamide / 12 h / Ambient temperature

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 83892-13-1
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

Guidance literature:: Multi-step reaction with 3 steps

1: HOBt, DCCI / ethyl acetate / 12 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 7 h

3: HOBt, DCCI / dimethylformamide / 12 h / Ambient temperature

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 83892-02-8
N-benzyloxycarbonyl-L-leucine butylamide

: 83892-13-1
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine butylamide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / methanol / 6 h

2: HOBt, DCCI / ethyl acetate / 12 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 7 h

4: HOBt, DCCI / dimethylformamide / 12 h / Ambient temperature

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;