Technology Process of C25H31NO4S
There total 3 articles about C25H31NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine;
In
1,4-dioxane;
at 100 ℃;
for 14h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2012.06.075
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
2: tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere
With
di-isopropyl azodicarboxylate; tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane;
1: Mitsunobu reaction / 2: Heck-aza-Michael reaction;
DOI:10.1016/j.tetlet.2012.06.075
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide / diethyl ether / -78 °C / Inert atmosphere
1.2: -60 - 20 °C
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
3.1: tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere
With
copper(l) iodide; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether;
2.1: Mitsunobu reaction / 3.1: Heck-aza-Michael reaction;
DOI:10.1016/j.tetlet.2012.06.075
