N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

Base Information

Chemical Name:N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine
CAS No.:1313372-14-3
Molecular Formula:C₄₇H₃₇N₃S
Molecular Weight:675.897
Hs Code.:

Synonyms:N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

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Chemical Property of N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

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Technology Process of N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

There total 5 articles about N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1313372-16-5
2-(5-bromothiophen-2-yl)-1-(4-(tert-butyl)phenyl)-1H-phenanthro-[9,10-d]imidazole

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1313372-14-3
N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; for 24h; Inert atmosphere; Reflux;
DOI:10.1039/c1jm10326a

Reference yield:

: 769-92-6
4-tert-Butylaniline

: 1313372-14-3
N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 24 h / Inert atmosphere; Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium carbonate; acetic acid; In ethanol; water; toluene; 2: Suzuki coupling;
DOI:10.1039/c1jm10326a

Reference yield:

: 4701-17-1
5-bromo-2-thiophencarboxaldehyde

: 1313372-14-3
N-(4-(5-(1-(4-tert-butylphenyl)-1H-phenanthro[9,10-d]-imidazol-2-yl)thiophen-2-yl)phenyl)-N-phenylbenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 24 h / Inert atmosphere; Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium carbonate; acetic acid; In ethanol; water; toluene; 2: Suzuki coupling;
DOI:10.1039/c1jm10326a