methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate

Base Information

• Chemical Name: methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate
• CAS No.: 1246371-75-4
• Molecular Formula: C₂₀H₂₀N₄O₃S
• Molecular Weight: 396.47

Synonyms:methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate

Chemical Property of methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate

Chemical Property:

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Technology Process of methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate

There total 1 articles about methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) + (5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetic acid hydrazide (49656-92-0) → methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate (1246371-75-4)

Guidance literature:

(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetic acid hydrazide; With hydrogenchloride; acetic acid; sodium nitrite; In water; at -5 ℃; for 0.25h;

glycine ethyl ester hydrochloride; With triethylamine; In ethyl acetate; at -5 - 25 ℃; for 48h;

DOI:10.3390/molecules15106759

Reference yield: 93.0%

methyl 2-[2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetylamino]-acetate (1246371-75-4) → N-(hydrazinocarbonylmethyl)-2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetamide (1246371-83-4)

Guidance literature:

With hydrazine hydrate; In ethanol; for 4h; Reflux;

DOI:10.3390/molecules15106759

upstream raw materials:

glycine ethyl ester hydrochloride

(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetic acid hydrazide

Downstream raw materials:

N-(hydrazinocarbonylmethyl)-2-(5-benzyl-4-phenyl-4H-[1,2,4]triazol-3-thio)-acetamide

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