12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

Base Information

Chemical Name:12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene
CAS No.:1357150-79-8
Molecular Formula:C₃₃H₃₂BNO₂
Molecular Weight:485.434
Hs Code.:

Synonyms:12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

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Chemical Property of 12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

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Technology Process of 12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

There total 9 articles about 12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1257220-44-2
7-bromo-12,12-dimethyl-10-phenyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 73183-34-3
bis(pinacol)diborane

: 1357150-79-8
12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; for 18h; Reflux;

Reference yield:

: 1257220-43-1
12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

: 1357150-79-8
12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / dimethyl sulfoxide / 12 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1257220-47-5
12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1357150-79-8
12,12-dimethyl-10-phenyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10,12-di hydro-10-azaindeno[2,1-b]fluorene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogensulfite; copper; 3,5-ditertbutyl salicylic acid; potassium carbonate / 10 h / 170 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide

3: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / dimethyl sulfoxide / 12 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 3,5-ditertbutyl salicylic acid; potassium acetate; copper; potassium carbonate; sodium hydrogensulfite; In dimethyl sulfoxide; N,N-dimethyl-formamide;