[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone

Base Information

• Chemical Name: [4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone
• CAS No.: 911836-46-9
• Molecular Formula: C₃₂H₃₈O₂
• Molecular Weight: 454.653

Synonyms:[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone

Chemical Property of [4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone

Chemical Property:

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Technology Process of [4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone

There total 1 articles about [4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

5-tert-Butyl-m-xylene (98-19-1) + terephthaloyl chloride (100-20-9) → [4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone (911836-46-9)

Guidance literature:

With aluminium trichloride; In nitrobenzene; for 1h;

DOI:10.1021/ol061505i

Reference yield: 96.0%

[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone (911836-46-9) → (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol (911836-47-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1.5h;

DOI:10.1021/ol061505i

Reference yield:

[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone (911836-46-9) → C61H68N4O7

Guidance literature:

Multi-step reaction with 4 steps

1: 96 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

2: 100 percent / aq. hydrobromic acid / 1 h / Heating

3: 93 percent / aq. ammonia / 1.5 h / 140 °C

4: triethylamine / CH₂Cl₂ / 20 °C

With ammonium hydroxide; lithium aluminium tetrahydride; hydrogen bromide; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol061505i

upstream raw materials:

5-tert-Butyl-m-xylene

terephthaloyl chloride

Downstream raw materials:

(4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol

C₃₂H₄₀Br₂

1,4-phenylenebis-[1-(4-tert-butyl-2,6-dimethylphenyl)methanamine]

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