sodium bis(2-hydroxyethyl)dithiocarbamate

Base Information

• Chemical Name: sodium bis(2-hydroxyethyl)dithiocarbamate
• CAS No.: 2801-04-9
• Molecular Formula: C5H11 N O2 S2 . Na
• Molecular Weight: 203.262
• Hs Code.: 2930909090
• Mol file: 2801-04-9.mol

Synonyms:Carbamicacid, bis(2-hydroxyethyl)dithio-, monosodium salt (8CI); Carbamodithioic acid,bis(2-hydroxyethyl)-, monosodium salt (9CI); SodiumN,N-bis(2-hydroxyethyl)aminodithiocarboxylate; SodiumN,N-bis(2-hydroxyethyl)dithiocarbamate; Sodiumbis(2-hydroxyethyl)dithiocarbamate

Chemical Property of sodium bis(2-hydroxyethyl)dithiocarbamate

Chemical Property:

• Vapor Pressure: 2.46E-05mmHg at 25°C
• Boiling Point: 321°C at 760 mmHg
• Flash Point: 148°C
• PSA: 75.79000
• LogP: -0.89520

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium bis(2-hydroxyethyl)dithiocarbamate

There total 3 articles about sodium bis(2-hydroxyethyl)dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,2'-iminobis[ethanol] (111-42-2) → sodium bis<2-hydroxyethyl>dithiocarbamate (2801-04-9)

Guidance literature:

With sodium hydroxide; In methanol; at 10 ℃; for 2h; under Ar or N₂ atmosphere;

DOI:10.1021/ac00283a012

Reference yield: 81.0%

carbon disulfide (75-15-0,12122-00-8) + 2,2'-iminobis[ethanol] (111-42-2) → sodium bis<2-hydroxyethyl>dithiocarbamate (2801-04-9)

Guidance literature:

2,2'-iminobis[ethanol]; With sodium hydroxide; In methanol; at 0 ℃; for 0.333333h;

carbon disulfide; In methanol; at 0 - 20 ℃; for 4h;

DOI:10.1021/jm300031j

Reference yield:

Tributyltin bis(2-hydroxyethyl)dithiocarbamate → sodium bis<2-hydroxyethyl>dithiocarbamate (2801-04-9)

Guidance literature:

With sodium hydrogensulfide; In methanol; at 4 ℃;

DOI:10.1021/jo00084a046

upstream raw materials:

carbon disulfide

2,2'-iminobis[ethanol]

Downstream raw materials:

[(C₆H₅)3SnS₂CN(CH₂CH₂OH)2]

Refernces

• 1、 Chen, Cheng,Yang, Ke-Wu,Zhai, Le,Ding, Huan-Huan,Chigan, Jia-Zhu. "Dithiocarbamates combined with copper for revitalizing meropenem efficacy against NDM-1-producing Carbapenem-resistant Enterobacteriaceae". supporting information. . Retrieved 2021/11/20.
• 2、 -. "CARBONIC ANHYDRASE INHIBITOR COMPRISING A DITHIOCARBAMATE". Page/Page column 21-22. . Retrieved 2013/04/24.