C₂₂H₂₇N₂O₃PS₅

Base Information

Chemical Name:C₂₂H₂₇N₂O₃PS₅
CAS No.:668483-75-8
Molecular Formula:C₂₂H₂₇N₂O₃PS₅
Molecular Weight:558.772
Hs Code.:

C<sub>22</sub>H<sub>27</sub>N<sub>2</sub>O<sub>3</sub>PS<sub>5</sub>

Synonyms:C₂₂H₂₇N₂O₃PS₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₇N₂O₃PS₅

Chemical Property:

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Technology Process of C₂₂H₂₇N₂O₃PS₅

There total 5 articles about C₂₂H₂₇N₂O₃PS₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 75-15-0,12122-00-8
carbon disulfide

: 77-78-1
dimethyl sulfate

: 668484-09-1
C₂₀H₂₅N₂O₃PS₃

: 668483-75-8
C₂₂H₂₇N₂O₃PS₅

Guidance literature:: carbon disulfide; C₂₀H₂₅N₂O₃PS₃; With sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

dimethyl sulfate; In water; dimethyl sulfoxide; for 3h;
DOI:10.1080/10426500307871

Reference yield:

: 19172-47-5,94367-93-8
Lawessons reagent

: 668483-75-8
C₂₂H₂₇N₂O₃PS₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: 63 percent / acetonitrile / 7 h / Heating

2.1: 89 percent / CH₃COONa / ethanol / 2 h / Heating

3.1: 73 percent / C₂H₅ONa / ethanol / 5 h / Heating

4.1: aq. NaOH / dimethylsulfoxide / 0.5 h / 20 °C

4.2: 63 percent / dimethylsulfoxide; H₂O / 3 h

With sodium hydroxide; sodium ethanolate; sodium acetate; In ethanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1080/10426500307871

Reference yield:

: 129224-53-9
2-cyano-2-cyclohexylidenethioacetamide

: 668483-75-8
C₂₂H₂₇N₂O₃PS₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: 63 percent / acetonitrile / 7 h / Heating

2.1: 89 percent / CH₃COONa / ethanol / 2 h / Heating

3.1: 73 percent / C₂H₅ONa / ethanol / 5 h / Heating

4.1: aq. NaOH / dimethylsulfoxide / 0.5 h / 20 °C

4.2: 63 percent / dimethylsulfoxide; H₂O / 3 h

With sodium hydroxide; sodium ethanolate; sodium acetate; In ethanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1080/10426500307871