Technology Process of C28H39NO7S2Si
There total 7 articles about C28H39NO7S2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thionyl chloride; triethylamine;
In
dichloromethane;
at 0 ℃;
for 0.5h;
DOI:10.1002/anie.201106205
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C
2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C
2.2: 0.67 h / 20 °C
3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere
4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C
5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C
With
dmap; thionyl chloride; methanesulfonamide; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide;
In
dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C
2: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C
With
thionyl chloride; methanesulfonamide; triethylamine;
In
dichloromethane; water; tert-butyl alcohol;
1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205
