1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

Base Information

Chemical Name:1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane
CAS No.:827347-45-5
Molecular Formula:C₂₄H₁₃BiCl₂F₆
Molecular Weight:695.244
Hs Code.:

Synonyms:1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

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Technology Process of 1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

There total 1 articles about 1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 160750-89-0
(4-F₃CC₆H₄)2BiCl

: 14658-94-7
1,3-dichloroazulene

: 827347-45-5
1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

Guidance literature:: With lithium 2,2,6,6-tetramethylpiperidide; In tetrahydrofuran; under Ar atm. to soln. lithium 2,2,6,6-tetramethylpiperidide in THF at -70°C soln. 1,3-dichloroazulene was added, soln. (4-F3CC6H4)2BiCl in THF was added and stirred for 5 min; elem. anal.;
DOI:10.1021/om040053f

Reference yield: 65.0%

: 13709-36-9
xenon difluoride

: 827347-45-5
1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuthane

: 827347-48-8
1,3-dichloro-2-azulenylbis(4-trifluoromethylphenyl)bismuth difluoride

Guidance literature:: In tetrahydrofuran; under Ar atm. to soln. Bi compound in THF XeF2 was added at 0°C, react. mixt. was stirred for 3 h; soln. was evapd., residue was crystd. from MeOH; elem. anal.;
DOI:10.1021/om040053f