methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

Base Information

Chemical Name:methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide
CAS No.:1255194-08-1
Molecular Formula:BrH*C₁₈H₁₇N₃O₄S
Molecular Weight:452.329
Hs Code.:

Synonyms:methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

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Technology Process of methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

There total 2 articles about methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 137104-37-1
methyl (Z)-2-(bromomethyl)-3-(4-nitrophenyl)-2-propenoate

: 103-85-5
monophenylthiourea

: 1255194-08-1
methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

Guidance literature:: In acetonitrile; at 25 ℃; for 1h;
DOI:10.3998/ark.5550190.0011.b24

Reference yield:

: 114106-93-3
methyl 2-[hydroxy(4-nitrophenyl)methyl]prop-2-enoate

: 1255194-08-1
methyl (Z)-3-(4-nitrophenyl)-2-[(N-phenylisothioureido)methyl]-2-propenoate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium bromide; sulfuric acid / acetonitrile / 25 °C

2: acetonitrile / 1 h / 25 °C

With sulfuric acid; lithium bromide; In acetonitrile;
DOI:10.1016/j.ejmech.2017.02.013