N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide

Base Information

• Chemical Name: N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide
• CAS No.: 153919-02-9
• Molecular Formula: C₂₉H₄₄N₂O₃S
• Molecular Weight: 500.746

Synonyms:N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide

Chemical Property of N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide

There total 1 articles about N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-2-cyano-6-phenyloxazolopiperidine (88056-92-2) → N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide (153919-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / Ambient temperature

2: 82 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;

DOI:10.1016/S0957-4166(00)80097-X

Reference yield: 98.0%

N-[(S)-1-((R)-2-Hydroxy-1-phenyl-ethyl)-piperidin-2-ylmethyl]-2,4,6-triisopropyl-benzenesulfonamide (153919-02-9) → 2,4,6-Triisopropyl-N-(S)-1-piperidin-2-ylmethyl-benzenesulfonamide

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1016/S0957-4166(00)80097-X

upstream raw materials:

(-)-2-cyano-6-phenyloxazolopiperidine

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