2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether

Base Information

• Chemical Name: 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether
• CAS No.: 77861-44-0
• Molecular Formula: C₁₄H₁₄N₄O₂S₂
• Molecular Weight: 334.423
• Mol file: 77861-44-0.mol

Synonyms:2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether

Chemical Property of 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether

There total 2 articles about 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dimethoxy-p-phenylenediamine (17626-02-7) → 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether (77861-44-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.85 g / ethanol / 1 h / Heating

2: 10 percent aq. HCl / 1 h / Heating

With hydrogenchloride; In ethanol;

DOI:10.1248/cpb.29.301

Reference yield:

2,5-bishydroquinone dimethylether (344343-02-8) → 2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether (77861-44-0)

Guidance literature:

With hydrogenchloride; for 1h; Heating;

DOI:10.1248/cpb.29.301

Reference yield:

2,5-bis(2-mercaptoimidazol-1-yl)hydroquinone dimethylether (77861-44-0) → 2,5-bis(imidazol-1-yl)hydroquinone dimethylether (77861-40-6)

Guidance literature:

With nitric acid; at 95 ℃; for 0.0833333h;

DOI:10.1248/cpb.29.301

upstream raw materials:

2,5-bishydroquinone dimethylether

2,5-dimethoxy-p-phenylenediamine

Downstream raw materials:

2,5-bis(imidazol-1-yl)hydroquinone dimethylether