3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

Base Information

Chemical Name:3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride
CAS No.:100287-22-7
Molecular Formula:C₂₉H₃₂N₄O₅*ClH
Molecular Weight:553.058
Hs Code.:

Synonyms:3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of 3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

There total 4 articles about 3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.7%

: 92406-42-3
3-cyclohexyl-1-methyl-1H-pyrazol-5-amine

: 62760-06-9
2-[1-(2-Nitro-phenyl)-meth-(E)-ylidene]-3-oxo-butyric acid 2-phenoxy-ethyl ester

: 100287-22-7
3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

Guidance literature:: In tert-butyl alcohol; at 80 ℃; for 24h;
DOI:10.1248/cpb.35.3235

Reference yield:

: 57582-44-2
2-phenoxyethyl acetoaceatate

: 100287-22-7
3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 94.4 percent / AcOH, piperidine / benzene / 24 h / 30 - 45 °C

2: 81.7 percent / 2-methyl-propan-2-ol / 24 h / 80 °C

With piperidine; acetic acid; In tert-butyl alcohol; benzene;
DOI:10.1248/cpb.35.3235

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 100287-22-7
3-Cyclohexyl-1,6-dimethyl-4-(2-nitro-phenyl)-4,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid 2-phenoxy-ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 94.4 percent / AcOH, piperidine / benzene / 24 h / 30 - 45 °C

2: 81.7 percent / 2-methyl-propan-2-ol / 24 h / 80 °C

With piperidine; acetic acid; In tert-butyl alcohol; benzene;
DOI:10.1248/cpb.35.3235