[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester

Base Information

• Chemical Name: [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester
• CAS No.: 88453-64-9
• Molecular Formula: C₃₀H₃₄O₇
• Molecular Weight: 506.596

Synonyms:[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester

Chemical Property of [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester

There total 3 articles about [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid tert-butyl ester (88453-87-6) → [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester (88453-64-9)

Guidance literature:

With hydrogenchloride; In methanol; at 50 ℃; for 1h;

DOI:10.1021/ja00316a048

Reference yield:

7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone (65131-09-1) + methyl <6-(3-(benzyloxy)pent-1-yl)-1-oxo-2-cyclohexen-5-yl>acetate (88453-63-8) → [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester (88453-64-9)

Guidance literature:

With lithium tert-butoxide; In tetrahydrofuran; 1.) r.t., 1h, reflux, 15 min.;

DOI:10.1021/ja00316a048

Reference yield:

7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone (65131-09-1) + methyl <6-(3-(benzyloxy)pent-1-yl)-1-oxo-2-cyclohexen-5-yl>acetate (88453-63-8) + lithium tert-butoxide (1907-33-1) → [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester (88453-64-9) + [3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid tert-butyl ester (88453-87-6)

Guidance literature:

With lithium tert-butoxide; In tetrahydrofuran; 1.) r.t., 1h, reflux, 15 min.;

DOI:10.1021/ja00316a048

upstream raw materials:

7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone

methyl <6-(3-(benzyloxy)pent-1-yl)-1-oxo-2-cyclohexen-5-yl>acetate

lithium tert-butoxide

[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid tert-butyl ester

Downstream raw materials:

methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

methyl 2-<3-(3-(benzyloxy)pent-1-yl)-4-hydroxy-5-methoxyanthraquinon-2-yl>acetate

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