7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE

Base Information

Chemical Name:7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE
CAS No.:65131-09-1
Molecular Formula:C15H12 O5 S
Molecular Weight:304.323
Hs Code.:2932209090
DSSTox Substance ID:DTXSID90449823
Nikkaji Number:J534.129I
Mol file:65131-09-1.mol

Synonyms:7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE;Methoxyphenylsulfonylisobenzofuranone

Suppliers and Price of 7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
7-Methoxy-3-phenylsulfonyl-1(3H)-isobenzofuranone
100mg
$ 110.00

TCI Chemical
7-Methoxy-3-phenylsulfonyl-1(3H)-isobenzofuranone >98.0%(HPLC)
1g
$ 231.00

Crysdot
7-Methoxy-3-(phenylsulfonyl)isobenzofuran-1(3H)-one 95+%
5g
$ 883.00

American Custom Chemicals Corporation
7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE 95.00%
5MG
$ 497.63

Alichem
7-Methoxy-3-(phenylsulfonyl)isobenzofuran-1(3H)-one
5g
$ 935.55

AK Scientific
7-Methoxy-3-phenylsulfonyl-1(3H)-isobenzofuranone
1g
$ 565.00

AHH
7-Methoxy-3-phenylsulfonyl-1(3H)-isobenzofuranone 97%
5g
$ 518.00

Total 9 raw suppliers

Chemical Property of 7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:186.0 to 190.0 °C
Refractive Index:1.613
Boiling Point:575.785°C at 760 mmHg
Flash Point:302.024°C
PSA：78.05000
Density:1.4g/cm³
LogP:3.41890
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:304.04054465
Heavy Atom Count:21
Complexity:489

Purity/Quality:

97% ^*data from raw suppliers

7-Methoxy-3-phenylsulfonyl-1(3H)-isobenzofuranone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC2=C1C(=O)OC2S(=O)(=O)C3=CC=CC=C3

Technology Process of 7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE

There total 8 articles about 7-METHOXY-3-PHENYLSULFONYL-1(3H)-ISOBENZOFURANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 73318-26-0
7-methoxy-3-(phenylthio)-1(3H)-isobenzofuranone

: 65131-09-1
7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone

Guidance literature:: With dihydrogen peroxide; In acetic acid; 1) RT, 2) reflux; m-chloroperbenzoic acid;
DOI:10.1021/jo01303a025

Reference yield: 72.0%

: phenylsulfone

: 73274-87-0,73713-38-9
3-hydroxy-7-methoxy-3H-isobenzofuran-1-one

: 65131-09-1
7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 6520-83-8
ethyl 2-methoxy-6-methylbenzoate

: 65131-09-1
7-methoxy-3-(phenylsulfonyl)-1(3H)-isobenzofuranone

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide, benzoyl peroxide / CCl₄ / Heating; Irradiation

2: 9percent HCl / acetic acid / 12 h / Heating

3: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

4: 98 percent / 30percent H₂O₂ / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid

With hydrogenchloride; N-Bromosuccinimide; Perbenzoic acid; dihydrogen peroxide; toluene-4-sulfonic acid; In tetrachloromethane; acetic acid; benzene;
DOI:10.1021/jo01303a025